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CasNo： 4389-45-1
MF： C8H9NO2
Appearance： pink to grey-brown crystalline powder
InChI:InChI=1/C8H9NO2/c1-5-3-2-4-6(7(5)9)8(10)11/h2-4H,9H2,1H3,(H,10,11)
The invention belongs to the technical f...
The present invention relates to a trans...
The present invention relates to the pro...
The present invention relates to two nov...
7-methyl-1H-indole-2,3-dione
3-methylantranilic acid
| Conditions | Yield |
|---|---|
|
With
sodium hydroxide; dihydrogen peroxide;
|
90% |
|
With
potassium chloride; dihydrogen peroxide; sodium hydroxide;
In
water;
at 0 - 20 ℃;
for 2.25h;
|
80% |
|
|
60% |
|
With
sodium hydroxide; dihydrogen peroxide;
at 85 - 90 ℃;
|
58% |
|
With
dihydrogen peroxide;
|
|
|
With
sodium perborate;
|
|
|
With
sodium hydroxide; potassium chloride; dihydrogen peroxide;
|
|
|
With
dihydrogen peroxide;
|
|
|
With
sodium hydroxide; dihydrogen peroxide;
|
|
|
With
dihydrogen peroxide; sodium hydroxide;
In
water;
at 0 - 50 ℃;
|
|
|
7-methyl-1H-indole-2,3-dione;
With
dihydrogen peroxide; sodium hydroxide;
In
water;
at 0 - 50 ℃;
for 0.5h;
With
hydrogenchloride;
In
water;
pH=4;
|
|
|
With
dihydrogen peroxide; sodium hydroxide;
In
water;
at 0 - 50 ℃;
for 0.5h;
|
|
|
With
sodium perborate;
|
|
|
With
dihydrogen peroxide;
|
|
|
Multi-step reaction with 2 steps
1: sodium hydroxide
With
sodium hydroxide;
|
|
|
With
dihydrogen peroxide; sodium hydroxide;
In
water;
at 80 ℃;
for 5.5h;
Inert atmosphere;
|
2-chloro-3-methylbenzoic acid
3-methylantranilic acid
| Conditions | Yield |
|---|---|
|
With
ammonia; sodium carbonate; copper(l) chloride;
In
dimethyl sulfoxide;
at 130 - 150 ℃;
for 5h;
|
93.1% |
7-methyl-1H-indole-2,3-dione
3-methyl-2-nitrobenzoic acid
8-methyl-3-o-tolyl-1H-quinazoline-2,4-dione
methanol
methyl 2-amino-3-methylbenzoate
2-Amino-3-methyl-benzoic acid propyl ester
2-amino-3-methyl-N-propylbenzamide
2-benzyl-5-methyl-1-naphthol
