CasNo： 83411-71-6
MF： C16H35O2P
InChI:InChI=1/C9H16N2/c1-2-3-4-5-7-11-8-6-10-9-11/h6,8-9H,2-5,7H2,1H3
The invention discloses a method for pre...
The invention discloses extraction agent...
Dialkylphosphinic acids were synthesised...
An improved process for production of di...
2,4,4-trimethyl-1-pentene
bis(2,4,4-trimethylpentyl)phosphinic acid
| Conditions | Yield |
|---|---|
|
With
sodium hypophosphite; di-tert-butyl peroxide; acetic acid;
In
N,N-dimethyl-formamide;
at 105 ℃;
Microwave irradiation;
|
83% |
|
With
di-tert-butyl peroxide; Octadecanethiol; hypophosphorous acid;
In
N,N-dimethyl-formamide;
at 120 ℃;
for 7h;
|
t-butylperoxy-2-ethyl hexanate
2,4-dimethylpentane
bis(2,4,4-trimethylpentyl)phosphinic acid
| Conditions | Yield |
|---|---|
|
With
hypophosphorous acid; hydrazine;
at 85 - 110 ℃;
for 56h;
under 0.2 - 0.4 Torr;
Inert atmosphere;
|
453 g |
N,N-dimethyl-formamide dimethyl acetal
2,4,4-trimethyl-1-pentene
2,4,4-trimethylpent-2-ene
bis(2,4,4-trimethylpentyl)monothiophosphinic chloride
(bis-2,4,4-trimethylpentyl)monothiophosphinic acid
